DETERMINATION OF THE ULTRA LONG RANGE SPIN-SPIN COUPLING CONSTANTS USING OVERALL LINE SHAPE ANALYSIS IN THE <sup>1</sup>H NMR SPECTRA OF FULLERENE-C<sub>60</sub> CYCLOADDUCTS WITH 1-(4-NITROPHENYL)-3-PHENYLNITRILE YLIDE

Authors

  • B. А. Чертков M. V. Lomonosov State University
  • C. В. Зубков M. V. Lomonosov State University
  • А. А. Овчаренко M. V. Lomonosov State University
  • А. B. Карчава M. V. Lomonosov State University
  • M. А. Юровская M. V. Lomonosov State University

DOI:

https://doi.org/10.1007/1069

Abstract

On the basis of the overall signal line shape in the 1H NMR spectra of [6,6]-closed and [5,6]-open fullerene-C60 cycloadducts with 1-(4-nitrophenyl)-3-phenylnitrile ylide we determined the values of the long range spin-spin coupling for the aliphatic proton of the heterocyclic fragment with the aromatic protons.

Authors: V. A. Chertkov, S. V. Zubkov, A. A. Ovcharenko, A. V. Karchava, and M. A. Yurovskaya.

English Translation in Chemistry of Heterocyclic Compounds, 1999, 35 (11), pp 1308-1312

http://link.springer.com/article/10.1007/BF02251999

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Published

2013-10-29

Issue

No. 11 (1999)

Section

Original Papers