COPPER-CATALYZED ARYLATION OF TETRAZOLE-5-THIONES UPON CONVECTION HEATING AND MICROWAVE ACTIVATION CONDITIONS

Authors

  • У. Н. Дмитриева St. Petersburg State Technological Institute (Technical University)
  • С. М. Рамш St. Petersburg State Technological Institute (Technical University)
  • Ю. Э. Зевацкий St. Petersburg State Technological Institute (Technical University)
  • Т. В. Артамонова St. Petersburg State Technological Institute (Technical University)
  • Л. В. Мызников St. Petersburg State Technological Institute (Technical University)

DOI:

https://doi.org/10.1007/1262

Keywords:

aryl iodide, cuprous chloride, ethylenediamine, tetrazole-5-thione, arylation, microwave activation

Abstract

The arylation of 1-phenyltetrazole-5-thione using a series of iodobenzene derivatives in the presence of cuprous chloride and a ligand such as ethylenediamine. It was shown that the use of microwave activation permitted shortening of the reaction time, increasing yields and simplification of the reaction products isolation.

Authors: U. N. Dmitrieva, S. M. Ramsh, Yu. E. Zevatskii, T. V. Artamonova, and L. V. Myznikov.

English translation in Chemistry of Heterocyclic Compounds, 2012, 48 (2), pp 355-357

http://link.springer.com/article/10.1007/s10593-012-0996-0

 

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Published

2013-11-29

Issue

No. 2 (2012)

Section

Original Papers