SYNTHESIS AND CRYSTAL STRUCTURE OF β-N-(5-METHYL-4-OXO-5,6-DIHYDRO-4H-1,3-THIAZIN-2-YL)ISONICOTINOHYDRAZIDE

Authors

  • И. В. Кулаков Institute of Organic Synthesis and Coal Chemistry of Kazakhstan Republic, Karaganda 100008
  • Д. М. Турдыбеков Research and Production Center "Phytochemistry", Ministry of Education and Science of the Republic of Kazakhstan, Karaganda 100009
  • О. А. Нуркенов Institute of Organic Synthesis and Coal Chemistry of Kazakhstan Republic, Karaganda 100008
  • Г. М. Исабаева Institute of Organic Synthesis and Coal Chemistry of Kazakhstan Republic, Karaganda 100008
  • А. С. Махмутова Research and Production Center "Phytochemistry", Ministry of Education and Science of the Republic of Kazakhstan, Karaganda 100009
  • К. М. Турдыбеков Research and Production Center "Phytochemistry", Ministry of Education and Science of the Republic of Kazakhstan, Karaganda 100009
  • С. Д. Фазылов Institute of Organic Synthesis and Coal Chemistry of Kazakhstan Republic, Karaganda 100008

DOI:

https://doi.org/10.1007/6589

Keywords:

methacryloylthiosemicarbazide of isonicotinic acid, intramolecular heterocyclization, X-ray crystallography

Abstract

In the presence of amines under mild conditions, β-N-(methacryloylcarbamoythioyl)isonicotinohydrazide underwent intramolecular heterocyclization to give  β-N-(5-methyl-4-oxo-5,6-dihydro-4H-1,3-thiazin-2-yl)isonicotinohydrazide, the spatial structure was confirmed by X-ray crystallography.

How to Cite
Kulakov, I. V.; Turdybekov, D. M.; Nurkenov, O. A.; Issabaeva, G. M.; Makhmutova, A. S.;Turdybekov, K. M.; Fazylov, S. D. Chem. Heterocycl. Compd. 2009, 45, 1117. [Khim. Geterotsikl. Soedin. 2009, 1395.]

For this article in the English edition see DOI 10.1007/s10593-009-0398-0

 

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Published

2022-02-14

Issue

No. 9 (2009)

Section

Original Papers