4-HYDROXY-2-QUINOLONES. 137. SYNTHESIS, STRUCTURE, AND SPECTROSCOPIC CHARACTERISTICS OF DIETHYL 2,2'-DIOXO-1,2,3,4,1',2',3',4'-OCTAHYDRO[4,4']BIQUINOLINYL-3,3'-DICARBOXYLATE

Authors

  • И. В. Украинец National University of Pharmacy, Kharkiv 61002
  • А. А. Ткач National University of Pharmacy, Kharkiv 61002
  • В. В. Кравцова National University of Pharmacy, Kharkiv 61002
  • А. В. Туров Taras Shevchenko National University, Kiev 01033

DOI:

https://doi.org/10.1007/7312

Keywords:

4-chloro-2-oxo-1, 2-dihydroquinolines, reductive dehalogenation, X-ray analysis

Abstract

Treatment of the ethyl esters of 1-R-4-chloro-2-oxo-1,2-dihydroquinoline-3-carboxylic acids with zinc 
dust in glacial acetic acid gives high yields  of diethyl 2,2'-dioxo-1,2,3,4,1',2',3',4'-octahydro[4,4']biquinolinyl-3,3'-dicarboxylates. The structural features of the synthesized compounds together with their NMR and mass spectra are discussed.

How to Cite
Ukrainets, I. V.; Tkach, A. A.; Kravtsova, V. V.; Turov, A. V.  Chem. Heterocycl. Compd. 2007, 43, 1525. [Khim. Geterotsikl. Soedin. 2007, 1799.]

For this article in the English edition see DOI 10.1007/s10593-007-0236-1


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Published

2023-01-13

Issue

No. 12 (2007)

Section

Original Papers