FACILE SYNTHESIS OF NEW (<i>Z</i>)-6-ARYLMETHYLIDENE-1,3,4-THIADIAZIN-5(6<i>H</i>)-ONE DERIVATIVES
DOI:
https://doi.org/10.1007/891Keywords:
N'-arylacetonitrilimines, (Z)-6-arylmethylidene-1, 3, 4-thiadiazin-5(6H)-one derivatives, 3-aryl-2-sulfanylpropenoic acidsAbstract
3-Aryl-2-sulfanylpropenoic acids reacted with acetohydrazonyl chlorides in refluxing absolute ethanol in the presence of equimolar amount of triethylamine forming (Z)-6-arylmethylidene-1,3,4-thiadiazin-5-one derivatives. X-Ray study on the crystal of one of the obtained products was carried out.
Also published in Chemistry of Heterocyclic Compounds, 2012, 48 (11), pp 1696-1700
http://link.springer.com/article/10.1007/s10593-013-1195-3