Synthesis and properties of N-methylmorpholinium 4aryl-6-methyl-5-phenylcarbamoyl-3cyano-1,4dihydropyridine-2-thiolates. Molecular and crystalline structure of 2allylthio-6-methyl-5-phenylcarbamoyl-4-(2chlorophenyl)-3-cyano-1,4-dihydropyridine

Authors

  • B. Д. Дяченко T. G. Shevchenko Lugansk State Pedagogical Institute, Lugansk 348011
  • C. Г. Кривоколыско T. G. Shevchenko Lugansk State Pedagogical Institute, Lugansk 348011
  • B. Н. Нестеров A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow 117813
  • B. П. Литвинов N. D. Zelinskii Institute of Organic Chemistry, Russian Academy of Sciences, 117913 Moscow

Abstract

By the condensation of an aromatic aldehyde, the anilide of acetoacetic acid, cyanothioacetamide, and Nmethylmorpholine, substituted N-methylmorpholinium 1,4-dihydropyridine-2-thiolates have been synthesized and subsequently used in the synthesis of the corresponding thiones, 2-alkylthiopyridines, thieno[2,3-b]pyridines, and disulfides. X-ray diffraction has been used to establish the structure of 2-allylthio-6-methyl-5-phenylcarbamoyl-4-(2-chlorophenyl)-3-cyano-1, 4-dihydropyridine.

How to Cite
Dyachenko, V. D.; Krivokolysko, S.;G.; Nesterov, V. N.; Litvinov, V. P. Chem. Heterocycl. Compd. 1996, 32, 1066. [Khim. Geterotsikl. Soedin. 1996, 1243.]

For this article in the English edition, see DOI https://doi.org/10.1007/BF01164714

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Published

1996-09-25

Issue

No. 9 (1996)

Section

Original Papers