NEW METHODS FOR THE SYNTHESIS OF α,ω-BIS-1,5,3-DITHIAZEPANES ON THE BASIS OF ALIPHATIC α,ω-DIAMINES

Authors

  • Е. Б. Рахимова Institute of Petrochemistry and Catalysis, Russian Academy of Sciences
  • Р. A. Исмагилов Ufa State University of Economics and Services
  • Р. A. Зайнуллин Ufa State University of Economics and Services
  • А. Г. Ибрагимов Institute of Petrochemistry and Catalysis, Russian Academy of Sciences
  • У. М. Джемилев Institute of Petrochemistry and Catalysis, Russian Academy of Sciences

DOI:

https://doi.org/10.1007/482

Keywords:

α, ω-bis-1, 5, 3-dithiazepanes, ω-diamines, catalysis, heterocyclization

Abstract

Efficient methods for the synthesis of α,ω-bis-1,5,3-dithiazepanes based on the heterocyclization of α,ω-diamines with N1,N1,N6,N6-tetramethyl-2,5-dithiahexane-1,6-diamine and on the intermolecular cyclization of 1,2-ethanedithiol with tetrakis(methoxymethyl)diamines catalyzed by SmCl3·6H2O have been developed.

Authors: E. B. Rakhimova, R. A. Ismagilov, R. A. Zainullin, A. G. Ibragimov, and U. M. Dzhemilev.

English Translation in Chemistry of Heterocyclic Compounds, 2013, 49 (8), pp 1237-1242

http://link.springer.com/article/10.1007/s10593-013-1368-0

Author Biographies

Е. Б. Рахимова, Institute of Petrochemistry and Catalysis, Russian Academy of Sciences

Елена Борисовна Рахимова

к.х.н., н.с. лаборатории гетероатомных соединений ИНК РАН

Р. A. Исмагилов, Ufa State University of Economics and Services

Ринат Арфикович Исмагилов

Р. A. Зайнуллин, Ufa State University of Economics and Services

Радик Анварович Зайнуллин

А. Г. Ибрагимов, Institute of Petrochemistry and Catalysis, Russian Academy of Sciences

Асхат Габдрахманович Ибрагимов

У. М. Джемилев, Institute of Petrochemistry and Catalysis, Russian Academy of Sciences

Усеин Меметович Джемилев

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Published

2013-06-17

Issue

No. 8 (2013)

Section

Original Papers