Synthesis and NMR spectroscopic study of derivatives of pyrazolo[1,5-<i>a</i>]pyrimidines

Authors

  • B. А. Макаров Center for the Chemistry of Medicinals, All-Russian Chemico-Pharmaceutical Scientific Research Institute, Moscow 119815
  • Н. П. Соловьева Center for the Chemistry of Medicinals, All-Russian Chemico-Pharmaceutical Scientific Research Institute, Moscow 119815
  • B. Г. Грaник Center for the Chemistry of Medicinals, All-Russian Chemico-Pharmaceutical Scientific Research Institute, Moscow 119815

Abstract

Reactions of 3,5-diamino-4-nitropyrazole with asymmetric β-dicarbonyl compounds formed pyrazolo[1,5-a]pyrimidines, which in turn were used as the starting compounds in the reaction with dimethylformamide diethylacetal. The structure of the compounds obtained was studied by NMR spectroscopy in experiments involving the homonuclear Overhauser effect.

How to Cite
Makarov, V. A.; Solov'eva, N. P; Granik, V. G. Chem. Heterocycl. Compd. 1997, 33, 535. [Khim. Geterotsikl. Soedin. 1997, 619.]

For this article in the English edition, see DOI https://doi.org/10.1007/BF02291935

Published

1997-05-25

Issue

Section

Original Papers